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directions found in The Journal of the American Chemical Society
Volume 60, page 1325 (1938). Propionic acid will never be a
restricted chemical because it has such wide use as a means to kill
fungus and mold growing on stored grain.
To do the reaction, a 250 ml flask and a dropping funnel are first
thoroughly dried, then a magnetic stirring bar is placed in the flask,
followed by 16 ml of pyridine and 25 ml of benzene. If there is a
question as to whether the pyridine or benzene are completely free of
Practical LSD Manufacture
68
water, the pryridine should be dried by adding some KOH pellets to
the jug of pyridine, and the benzene dried azeotropically by distilling
off 10% of it, and using the residue.
Now to the stirred solution, rapidly add 9.25 grams (8.75 ml) of
propionyl chloride. This causes a small rise in temperature, and
pyridium complex conies out of solution. Then, with continued
stirring, add 7.4 grams (7.4 ml) of propionic acid over a period of 5
minutes from a dropping funnel. This causes the solution to get hot,
and pyridine hydrochloride comes out of solution.
The stirring is continued for an additional 10 minutes, then the
pyridine hydrochloride is filtered out in a Buchner funnel. This should be
done rapidly, and on a dry day, because the pyridine hydrochloride is
very hygroscopic, and will melt. The filter cake of pyridine
hydrochloride should then be quickly rinsed with dry benzene, and the
combined filtrate should be concentrated under a vacuum, using
steam or hot water to heat the flask. When the benzene and pyridine
have distilled off, they will be followed by the product, propionic
anhydride, boiling at about 70° C under a typical aspirator vacuum of 20
torr. This product may be contaminated with some propionic acid, and
it can be removed by redistilling the product through a
fractionating column, either at normal pressure or under a vacuum.
Propionic acid boils at 141° C, while the anhydride boils at 168° C at
normal pressure.
10 Solvent
Management
69
10 Solvent Management
A cursory reading of this text will make it plain to everyone that
the production of LSD involves heavy usage of solvents. From the
defatting and extraction of the crops to the crystallization of pure
LSD, a variety of solvents must be used in large amounts relative to
the product to get a fairly pure product.
"Fairly pure product"... how we starved masses long for such a
thing. Back in the 70s when I dropped my first doses of acid, the
stories were already impossibly ingrained in the consuming public's
mind that the acid was cut with speed or strychnine. All of the stories
are easily disproved, yet they persist to this day. If the entire weight of a
blotter paper was made of pure meth or strychnine, its effect would be
less than pronounced. The truth of the matter is that lysergicsimilar
compounds contaminating the LSD are responsible for these
undesirable effects. From clavine alkaloids to unh
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sexual aphrodisiac The researchers claim that this is the first time that a causal connection between migraine and major depression has been established that results from bidirectional influences. This means that each disorder increases the risk for first onset of the other. In other words, having depression predisposes one to migraine, and vice versa. This undermines the idea that the connection is psychological - an explanation that would be plausible only if the researchers had found a one-directional effect from migraine to depression. The researchers concluded that there is no simple explanation for the migraine/depression connection and that it is probably biochemical in nature, indicating that supplementation is a plausible solution.
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directions found in The Journal of the American Chemical Society
Volume 60, page 1325 (1938). Propionic acid will never be a
restricted chemical because it has such wide use as a means to kill
fungus and mold growing on stored grain.
To do the reaction, a 250 ml flask and a dropping funnel are first
thoroughly dried, then a magnetic stirring bar is placed in the flask,
followed by 16 ml of pyridine and 25 ml of benzene. If there is a
question as to whether the pyridine or benzene are completely free of
Practical LSD Manufacture
68
water, the pryridine should be dried by adding some KOH pellets to
the jug of pyridine, and the benzene dried azeotropically by distilling
off 10% of it, and using the residue.
Now to the stirred solution, rapidly add 9.25 grams (8.75 ml) of
propionyl chloride. This causes a small rise in temperature, and
pyridium complex conies out of solution. Then, with continued
stirring, add 7.4 grams (7.4 ml) of propionic acid over a period of 5
minutes from a dropping funnel. This causes the solution to get hot,
and pyridine hydrochloride comes out of solution.
The stirring is continued for an additional 10 minutes, then the
pyridine hydrochloride is filtered out in a Buchner funnel. This should be
done rapidly, and on a dry day, because the pyridine hydrochloride is
very hygroscopic, and will melt. The filter cake of pyridine
hydrochloride should then be quickly rinsed with dry benzene, and the
combined filtrate should be concentrated under a vacuum, using
steam or hot water to heat the flask. When the benzene and pyridine
have distilled off, they will be followed by the product, propionic
anhydride, boiling at about 70° C under a typical aspirator vacuum of 20
torr. This product may be contaminated with some propionic acid, and
it can be removed by redistilling the product through a
fractionating column, either at normal pressure or under a vacuum.
Propionic acid boils at 141° C, while the anhydride boils at 168° C at
normal pressure.
10 Solvent
Management
69
10 Solvent Management
A cursory reading of this text will make it plain to everyone that
the production of LSD involves heavy usage of solvents. From the
defatting and extraction of the crops to the crystallization of pure
LSD, a variety of solvents must be used in large amounts relative to
the product to get a fairly pure product.
"Fairly pure product"... how we starved masses long for such a
thing. Back in the 70s when I dropped my first doses of acid, the
stories were already impossibly ingrained in the consuming public's
mind that the acid was cut with speed or strychnine. All of the stories
are easily disproved, yet they persist to this day. If the entire weight of a
blotter paper was made of pure meth or strychnine, its effect would be
less than pronounced. The truth of the matter is that lysergicsimilar
compounds contaminating the LSD are responsible for these
undesirable effects. From clavine alkaloids to unh
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The researchers claim that this is the first time that a causal connection between migraine and major depression has been established that results from bidirectional influences.
This means that each Female Aphrodisiac disorder increases the risk for first onset of the other. In other words, having depression predisposes one to migraine, and vice versa. This undermines the idea that the connection is psychological - an explanation that would be plausible only if the researchers had found a one-directional effect from migraine to depression. The researchers concluded that there is no simple explanation for the migraine/depression connection and that it is probably biochemical in nature, indicating that supplementation is a plausible solution.
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Sex ved immeasurably. Partners in crime
are too easily turned against you and transformed into star witnesses.
Don't deceive yourself by thinking that your friends would never do
such a thing. This country is populated with sheeple who lick the
boots of their masters at the drop of a hat. The added incentive of
avoiding jail time turns these bleating sheeple into singing stool
pigeons nearly every time.
Along with partners in crime, one's customers for the product are a
prime source of snitches. The first and foremost rule in contacts with
one's customers is that they have no business knowing that you are
cooking the product yourself. The reason for this, beyond their
babbling their mouths to their friends, is that if they get themselves
into trouble they then have a lot more leverage for cutting themselves a
snitching bargain with the heat if they say that they can deliver up an
LSD lab. More leverage for them turns into more time and freedom
Practical LSD Manufacture
72
for this turncoat to work at setting you up, because the heat sees a
bigger pot of gold at the end of the rainbow. If all he has to offer to the
heat is just another LSD connection, they will get frustrated with him if
he does not immediately deliver on your demise, and will put his
squealing butt in the slam where it belongs.
Several further tactics are called for to protect yourself from
treachery emanating from your customers. If the heat succeeds in
turning your customer against you, they will first try to get themselves in
on a transaction, and failing this, try to make what is called a
"controlled buy" whereby thek traitor buys while they watch and
maybe record.
To foil such tactics, you must be in control of setting up
transactions, not your customers. They do not call you to set up deals; in
fact, it's best that they not even have your number, address or real
name. Know well the schedules and habits of your customers, and
simply call them with very short warning times of your arrival and
readiness to do business. Third parties are not invited, wanted or
allowed. If they don't have all the cash ready at hand, just front the
remainder with an understanding of how long it will take to gather up
the balance. Then return similarly unannounced to collect what is
owed. By this I don't mean to come back in a couple hours to pick up
the marked bills. Rather, the time frame must be sufficiently long so as
to make a stake-out by the enemy a real pain and not worth their
bother.
Explicit telephone conversations with one's customers are a
definite no-no, and such an understanding must be reached with them
from the outset. Rather, the conversations should be friendly, filled
with small talk, and mostly held to make sure the guy is home. Use of
codewords and other such nonsense is for idiots. If one's customer
breaks these pre-agreed-upon rules, it is cause for suspicion.
The delivery machine of choice is a street-legal dirt bike. This
vehicl
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