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ydrolysed ergot
alkaloids, to unreacted lysergic acid, or lysergic acid hydrazides to iso-
LSD and God knows what substances created by the mishandling of
the raw materials and product, a contaminated product is much easier to
make than a pure one.
The use of large volumes of solvents poses twin problems:
obtaining them and disposing of them. Both problems are made vastly
Practical LSD Manufacture
70
simpler by recycling the solvents. Just because a solvent has been
used once in a given stage of the process does not mean its useful
lifetime is over. For example, the solvent used for defatting the crop is
easily made as good as new by distilling it to free it of its load of fat.
Other solvents are not so easily recovered for re-use because the
procedure calls for the given solvent to be removed from the product
by vacuum evaporation. In this case, the solvent can be collected in a
cold trap placed along the vacuum line on its way to the vacuum
source. If a pump is used to create the vacuum, such a trap is vital to
prevent solvent vapors from getting into the pump oil, thereby ruining
the lubrication and the vacuum created.
A cold trap can be constructed of either glass or steel; it need only be
large enough to hold the solvent collected, and airtight so as not to ruin
the vacuum with leaks. This cold trap is then cooled down with dry ice
during vacuum evaporations to condense the solvent vapors in the trap.
The solvent recovered in the trap can be re-used in the given stage of
the process from whence it came. I would not co-mingle recovered
solvents from different stages. For example, chloroform from the
alkaloid extraction of the crops should be kept for that usage, and not
be used for LSD crystallization, because it will also contain some
ammonia and methanol.
The recovery of ether, for example, from method 2 of lysergic acid
production, poses a special problem. This problem is the formation of
explosive peroxides in ether during storage. Ether containing water
and alcohol, as would be the case for this recovered solvent, does not
form much peroxide. There is a possibility that dry ether can be made
free of peroxides by shaking the ether with some 5% ferrous sulfate
(FeSO4) solution in water prior to distilling. Failure to do this may
expose the operator to a fiery explosion during distillation. Ice water
flowing through the condenser, and an ice-chilled receiving flask, are
required to get an efficient Aphrodisiac Perfume condensation of the ether during
distillation.
11
Keeping Out Of Trouble 71
II
Keeping Out Of Trouble
The dangers of LSD manufacturing do not end with the possibility
that the cooker may spill some of the stuff on himself and fry his
brain.
There is a much more malignant danger facing those who
embark upon this course: Johnny Law.
The conduit through which those shit-eating dogs travel to get to
you is your associates. If you are cooking alone with no partners in
crime, your safety has been impro
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Orexis Danger Yohimbe is a tree that grows throughout the African nations of Cameroon, Gabon and Zaire. (A similar plant in South America is called Quebracho). For centuries, natives from these areas have ingested both the crude bark and purified compound as a tonic to enhance sexual prowess and as an aphrodisiac. The bark has been smoked as a hallucinogen and has been used in traditional medicine to treat angina and hypertension. The herb is a sensual stimulant for healthy men and women. Today, doctors prescribe an extract from the tree to treat organic impotence.
Yohimbe's energizing effects stem from it's ability to increase blood flow to the genitals, both male and female. It is thought to stimulate the pelvic nerve ganglia and thus is helpful for men with erection problems. In fact a prescription drug, yohimbine hydrochloride, is the only FDA approved drug for impotence. Effects can include increased libido, increased sensation and increased stamina. Women have also reported similar effects and general pleasant sensations.
Yohimbe bark contains about 6% yohimbine. This constituent is an indole alkaloid that is classified as an alpha-2-adrenergic blocking agent. The herb has a general nervous system stimulatory effect and can cause changes in blood pressure by dilating blood vessels. It can increase the heart rate, raise body temperature and increase blood pressure. At higher dosages, it has a mild psychotropic effect.
Yohimbe bark stimulates chemical reactions in the body that may aid in psychogenic cases of impotence, due to fatigue, tension and stress. Clinical studies have shown the herb to be effective in restoring potency in diabetic and heart patients who suffer from impotency. As an alpha-adrenoreceptor blocker, yohimbe reduces the effect of hormones that cause constriction of blood vessels, which typically increases as we age. It increases the body's production of norepinephrine which is essential in the formation of erections. Yohimbe may also boost the adrenaline supply to nerve endings, which can quicken male sensual stimulation. It has been used in combination with ginseng and saw palmetto as a remedy for men with low sex drive.
Yohimbe is also a short term MAO (monoamine oxidase) inhibitor and should be used with caution, especially if you have high blood pressure. Being an MAO inhibitor, yohimbe should not be taken with any food or drink containing tyramines (cheese, chocolate, beer, aged meats, nuts, etc.) and particularly not with the amino acids tyrosine or phenylalanine. A rise in blood pressure can result from the body not being able to remove the tyramines from these foods. It may be dangerous if used with anti-depressants, sedatives, antihistamines, caffeine, or amphetamines. Yohimbe may have other side effects such as racing heart rate, irritability, headache, nausea, sweating, dizziness and frequent urination. Anyone with a heart condition, kidney disease, glaucoma or history of gastric or duodenal ulcers should avoid skiniks.net aphrodisiac skiniks.net Cancer Chemotherapy Chinese Detox Medicine
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has been reduced.
The Operation Julie cooker had made the obvious analogy that if
the procedure works for these substances closely related to LSD, it
should also work for LSD. This type of underground research and
discovery is not at all unusual. If you look through the Chem. Abstracts
for references to the use of hydriodic acid and red phosphorus in the
reduction of ephedrine to meth, you will find nothing. This procedure is
a general method of reducing alcohols to alkanes, and was applied by
clandestine chemists to ephedrine with excellent results. Ditto for the
lithium-metal-in-liquid-ammonia reduction of ephedrine to meth.
To get the full details of the following procedure, your command of
Russian or Hungarian had better be firmer than mine. All this research
came out of Eastern Europe. For example, see Chem. Abstracts,
Volume 93, column 186636. This will then direct you to: Otkrytiya,
hobret., Prom. Obraztsy, Tovarnye Znaki 1980, (19), 303. Also Italian
patent application 76/50,746 dating to Dec. 6, 1976.
For this method to be superior to the procedures given in the
earlier chapters of this book, the need for a close stoichiometric
quantity of anhydride added would have to be done away with. It must be
possible to add a healthy excess of the propionic anhydride to get
100% conversion of the lysergic acid to the mixed anhydride. It would
Method X 67
further be nice if the procedure works with the hydrous form of
lysergic acid, doing away with the need to bake it under high vacuum.
Further advances in LSD manufacture taken from analogy to
closely related compounds can also be found in the hydrazide "one-pot
shot" route to LSD. It would appear that lysergic acid hydrazide can
be reacted with the very common chemical sodium nitrite, and then
diethylamine to give LSD. This eliminates the need to synthesize or
otherwise obtain 2,4-pentanedione.
(For synthesis of 2,4-
pentanedione, see U.S. Patent 2,737,528 and 2,834,811.) See Chem.
Abstracts Volume 94, column 209051 (1981) and German Patent
2,924,102. Another analogy can be found in Chem. Abstracts Volume
99, column 71069 which then refers you to German Patent DE
3,239,788. It would appear that phosgene, as used in Chapter 8, can be
replaced with oxalyl chloride. This substance is much less
dangerous than phosgene, and more easily measured History Of Aphrodisiac out.
Preparation of Propionic Anhydride
Propionic anhydride is obviously going to be impossible to
purchase without getting busted.
It is, however, not too difficult to
make in good yield and high purity. The simplest method of
preparation is via the general method found on page 28 of Organic
Synthesis Collective Volume 3. In Olfactory Aphrodisiac this method propionic acid reacts
with propionyl chloride in the presence of pyridine to yield propionic
anhydride. Propionyl chloride is at present an easily obtained
substance, but in the future, this may change. When that time comes,
propionyl chloride can be easily made from propionic acid b
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y the
directions found in The Journal of the American Chemical Society
Volume 60, page 1325 (1938). Propionic acid will never be a
restricted chemical because it has such wide use as a means to kill
fungus and mold growing on stored grain.
To do the reaction, a 250 ml flask and a dropping funnel are first
thoroughly dried, then a magnetic stirring bar is placed in the flask,
followed by 16 ml of pyridine and 25 ml of benzene. If there is a
question as to whether the pyridine or benzene are completely free of
Practical LSD Manufacture
68
water, the pryridine should be dried by adding some KOH pellets to
the jug of pyridine, and the benzene dried azeotropically by distilling
off 10% of it, and using the residue.
Now to the stirred solution, rapidly add 9.25 grams (8.75 ml) of
propionyl chloride. This causes a small rise in temperature, and
pyridium complex conies out of solution. Then, with continued
stirring, add 7.4 grams (7.4 ml) of propionic acid over a period of 5
minutes from a dropping funnel. This causes the solution to get hot,
and pyridine hydrochloride comes out of solution.
The stirring is continued for an additional 10 minutes, then the
pyridine hydrochloride is filtered out in a Buchner funnel. This should be
done rapidly, and on a dry day, because the pyridine hydrochloride is
very hygroscopic, and will melt. The filter cake of pyridine
hydrochloride should then be quickly rinsed with dry benzene, and the
combined filtrate should be concentrated under a vacuum, using
steam or hot water to heat the flask. When the benzene and pyridine
have distilled off, they will be followed by the product, propionic
anhydride, boiling at about 70° C under a typical aspirator vacuum of 20
torr. This product may be contaminated with some propionic acid, and
it can be removed by redistilling the product through a
fractionating column, either at normal pressure or under a vacuum.
Propionic acid boils at 141° C, while the anhydride boils at 168° C at
normal pressure.
10 Solvent
Management
69
10 Solvent Management
A cursory reading of this text will make it plain to everyone that
the production of LSD involves heavy usage of solvents. From the
defatting and extraction of the crops to the crystallization of pure
LSD, a variety of solvents must be used in large amounts relative to
the product to get a fairly pure product.
"Fairly pure product"... how we starved masses long for such a
thing. Back in the 70s when I dropped my first doses of acid, the
stories were already impossibly ingrained in the consuming public's
mind that the acid was cut with speed or strychnine. All of the stories
are easily disproved, yet they persist to this day. If the entire weight of a
blotter paper was made of pure meth or strychnine, its effect would be
less than pronounced. The truth of the matter is that lysergicsimilar
compounds contaminating the LSD are responsible for these
undesirable effects. From clavine alkaloids to unh
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are too easily turned against you and transformed into star witnesses.
Don't deceive yourself by thinking that your friends would never do
such a thing.
maca root and yohimbe
This country is populated with sheeple who lick the
boots of their masters at the drop of a hat. The added incentive of
avoiding jail time turns these bleating sheeple into singing stool
pigeons nearly every time.
Along with partners in crime, one's customers for the product are a
prime source of snitches. The first and foremost rule in contacts with
one's customers is that they have no business knowing
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cooking the product yourself. The reason for this, beyond their
babbling their mouths to their friends, is that if they get themselves
into trouble they then have a lot more leverage for cutting themselves a
snitching bargain with the heat if they say that they can deliver up an
LSD lab. More leverage for them turns into more time and freedom
Practical LSD Manufacture
72
for this turncoat to work at setting you up, because the
heat sees a
bigger pot of gold at the end of the rainbow. If all he has to offer to the
heat is just another LSD connection, they will get frustrated with him if
he does not immediately deliver on your demise, and will put his
squealing butt in the slam where it belongs.
Several further tactics are called for to protect yourself from
treachery emanating from your customers.
If the heat succeeds in
turning your customer against you, they will first try to get themselves in
on a transaction, and failing this, try to make what is called a
"controlled buy" whereby thek traitor buys while they watch and
maybe record.
To foil such tactics, you must be in control of setting up
transactions, not your customers. They do not call you to set up deals; in
fact, it's best that they not even have your number, address or real
name.
Know well the schedules and habits of your customers, and
simply call them with very short warning times of your arrival and
readiness to do business. Third parties are not invited, wanted or
allowed. If they don't have all the cash ready at hand, just front the
remainder with an understanding of how long it will take to gather up
the balance. Then return similarly unannounced to collect what is
owed. By this I don't mean to come back in a couple hours to pick up
the marked bills. Rather, the time frame must be sufficiently long so as
to make a stake-out by the enemy a real pain and not worth their
bother.
Explicit telephone conversations with one's customers are a
definite no-no, and such an understanding must be reached with them
from the outset.
Rather, the
maca root and yohimbe conversations should be friendly, filled
with small talk, and mostly held to make sure the guy is home. Use of
codewords and other such nonsense is for idiots. If one's customer
breaks these pre-agreed-upon rules, it is cause for suspicion.
The delivery machine of choice is a street-legal dirt bike. This
vehicl
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