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e is to be preferred because if the heat jumps you while on the
way to a delivery, you can take off and travel routes they can't through
backyards, ditches and cross-country, making a life-or-death drive for
the nearest body of water. If you're in the desert you deserve what you
11
Keeping Out Of Trouble 73
get for living where people aren't meant to be. Once a body of water is
reached, the contraband can then be disposed of. A proper excuse for
fleeing is that you thought they looked like a bunch of assassins. With
all the black-hooded ninja-wanna-be police these days, this is a most
believable excuse.
Setting up shop and getting chemicals is another source of
exposure to the forces of our enemy, the state. See the "Love Letters
from the Heat" section at the end of the book. Listed there are the
required snitch-list chemicals. A series
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of tactics are
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circumvent the reporting requirements. Sensitive chemicals are homesynthesized
according to the directions given in this book. The fivefinger-
discount method of acquisition is practiced to the fullest extent
possible at work or school to obtain chemicals and equipment. Where an
inside job will not yield the desired results, an actual heist at some plant
may be called for. This is a reasonable course of action only if you
know through a person inside the target about the availability of desired
items, and the presence of security measures. Burglary is not the sort of
thing to do hit-and-miss.
Other good sources of
Antioxidant Aphrodisiac Skiniks Net Vaginal equipment and chemicals are the surplus
market and waste exchanges. Dealers in the surplus market can be
found in trade publications for the chemical industry and those
industries which use a lot of chemicals.
The surplus people buy the
chemical stock of defunct businesses, or chemicals no longer wanted by
other businesses, and re-sell them. The typical surplus dealer is more
concerned with moving his stock than with brown-nosing the feds. A
company letterhead and a phone will open the door to most of these
people.
The waste exchanges came about as a result of hazardous-waste
laws which prevent the dumping of chemical waste and unused
chemicals. The waste exchanges act as matchmakers to bring together
those with unwanted chemicals and those who want them. A list of
waste exchanges is included at the back of this book. A company
letterhead gets you into the waste exchange network, a world filled
with eager chemical-holders who will generally send you their
chemicals if you pay shipping.
Practical LSD Manufacture
74
When these measures fail, setting up a front operation using
chemicals opens the legitimate pipeline to your door. One such
business which can be founded and then subverted to the needs of
LSD synthesis is metal plating. From the stocking of plating baths, to
analytical chemicals to monitor the composition of these baths, to
waste water treatment chemicals, the electroplating field is awash
with chemicals useful for making
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alkaloids, to unreacted lysergic acid, or lysergic acid hydrazides to iso-
LSD and God knows what substances created by the mishandling of
the raw materials and product, a contaminated product is much easier to
make than a pure one.
The use of large volumes of solvents poses twin problems:
obtaining them and disposing of them. Both problems are made vastly
Practical LSD Manufacture
70
simpler by recycling the solvents. Just because a solvent has been
used once in a given stage of the process does not mean its useful
lifetime is over. For example, the solvent used for defatting the crop is
easily made as good as new by distilling it to free it of its load of fat.
Other solvents are not so easily recovered for re-use because the
procedure calls for the given solvent to be removed from the product
by vacuum evaporation. In this case, the solvent can be collected in a
cold trap placed along the vacuum line on its way to the vacuum
source. If a pump is used to create the vacuum, such a trap is vital to
prevent solvent vapors from getting into the pump oil, thereby ruining
the lubrication and the vacuum created.
A cold trap can be constructed of either glass or steel; it need only be
large enough to hold the solvent collected, and airtight so as not to ruin
the vacuum with leaks. This cold trap is then cooled down with dry ice
during vacuum evaporations to condense the solvent vapors in the trap.
The solvent recovered in the trap can be re-used in the given stage of
the process from whence it came. I would not co-mingle recovered
solvents from different stages. For example, chloroform from the
alkaloid extraction of the crops should be kept for that usage, and not
be used for LSD crystallization, because it will also contain some
ammonia and methanol.
The recovery of ether, for example, from method 2 of lysergic acid
production, poses a special problem. This problem is the formation of
explosive peroxides in ether during storage. Ether containing water
and alcohol, as would be the case for this recovered solvent, does not
form much peroxide. There is a possibility that dry ether can be made
free of peroxides by shaking the ether with some 5% ferrous sulfate
(FeSO4) solution in water prior to distilling. Failure to do this may
expose the operator to a fiery explosion during distillation. Ice water
flowing through the condenser, and an ice-chilled receiving flask, are
required to get an efficient condensation of the ether during
distillation.
11
Keeping Out Of Trouble 71
II
Keeping Out Of Trouble
The dangers of LSD manufacturing do not end with the possibility
that the cooker may spill some of the stuff on himself and fry his
brain. There is a much more malignant danger facing those who
embark upon this course: Johnny Law.
The conduit through which those shit-eating dogs travel to get to
you is your associates. If you are cooking alone with no partners in
crime, your safety has been impro
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The only side effect reported by the subjects taking 5-HTP was stomachache, of which there were 41 instances during the entire three-year trial. In the placebo group, there were only 10 instances of stomachache, but also 118 instances of nausea and 78 of abdominal pain. This is not inconsistent with the very few side effects other studies have reported by those taking 5-HTP. These results may be explained by 5-HTP's ability to reduce hypersensitivity to pain. Moreover, in the study, eosinophilia (elevation of the special white blood cells associated with inflammation) was not reported in the 5-HTP group; in the control group, there was one case.
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The Operation Julie cooker had made the obvious analogy that if
the procedure works for these substances closely related to LSD, it
should also work for LSD. This type of underground research and
discovery is not at all unusual. If you look through the Chem. Abstracts
for references to the use of hydriodic acid and red phosphorus in the
reduction of ephedrine to meth, you will find nothing. This procedure is
a general method of Spanish Fly Aphrodisiac reducing alcohols to alkanes, and was applied by
clandestine chemists to ephedrine with excellent results. Ditto for the
lithium-metal-in-liquid-ammonia reduction of ephedrine to meth.
To get the full details of the following procedure, your command of
Russian or Hungarian had better be firmer than mine. All this research
came out of Eastern Europe. For example, see Chem. Abstracts,
Volume 93, column 186636. This will then direct you to: Otkrytiya,
hobret., Prom. Obraztsy, Tovarnye Znaki 1980, (19), 303. Also Italian
patent application 76/50,746 dating to Dec. 6, 1976.
For this method to be superior to the procedures given in the
earlier chapters of this book, the need for a close stoichiometric
quantity of anhydride added would have to be done away with. It must be
possible to add a healthy excess of the propionic anhydride to get
100% conversion of the lysergic acid to the mixed anhydride. It would
Method X 67
further be nice if the procedure works with the hydrous form of
lysergic acid, doing away with the need to bake it under high vacuum.
Further advances in LSD manufacture taken from analogy to
closely related compounds can also be found in the hydrazide "one-pot
shot" route to LSD. It would appear that lysergic acid hydrazide can
be reacted with the very common chemical sodium nitrite, and then
diethylamine to give LSD. This eliminates the need to synthesize or
otherwise obtain 2,4-pentanedione. (For synthesis of 2,4-
pentanedione, see U.S. Patent 2,737,528 and 2,834,811.
) See Chem.
Abstracts Volume 94, column 209051 (1981) and German Patent
2,924,102. Another analogy can be found in Chem. Abstracts Volume
99, column 71069 which then refers you to German Patent DE
3,239,788. It would appear that phosgene, as used in Chapter 8, can be
replaced with oxalyl chloride. This substance is much less
dangerous than phosgene, and more easily measured out.
Preparation of Propionic Anhydride
Propionic anhydride is obviously going to be impossible to
purchase without getting busted. It is, however, not too difficult to
make in good yield and high purity. The simplest method of
preparation is via the general method found on page 28 of Organic
Synthesis Collective Volume 3. In this method propionic acid reacts
with propionyl chloride in the presence of pyridine to yield propionic
anhydride. Propionyl chloride is at present an easily obtained
substance, but in the future, this may change. When that time comes,
propionyl chloride can be easily made from propionic acid b
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ved immeasurably. Partners in crime
are too easily turned against you and transformed into star witnesses.
Don't deceive yourself by thinking that your friends would never do
such a thing. This country is populated with sheeple who lick the
boots of their masters at the drop of a hat. The added incentive of
avoiding jail time turns these bleating sheeple into singing stool
pigeons nearly every time.
Along with partners in crime, one's customers for the product are a
prime source of snitches. The first and foremost rule in contacts with
one's customers is that they have no business knowing that you are
cooking the product yourself. The reason for this, beyond their
babbling their mouths to their friends, is that if they get themselves
into trouble they then have a lot more leverage for cutting themselves a
snitching bargain with the heat if they say that they can deliver up an
LSD lab. More leverage for them turns into more time and freedom
Practical LSD Manufacture
72
for this turncoat to work at setting you up, because the heat sees a
bigger pot of gold at the end of the rainbow. If all he has to offer to the
heat is just another LSD connection, they will get frustrated with him if
he does not immediately deliver on your demise, and will put his
squealing butt in the slam where it belongs.
Several further tactics are called for to protect yourself from
treachery emanating from your customers. If the heat succeeds in
turning your customer against you, they will first try to get themselves in
on a transaction, and failing this, try to make what is called a
"controlled buy" whereby thek traitor buys while they watch and
maybe record.
To foil such tactics, you must be in control of setting up
transactions, not your customers. They do not call you to set up deals; in
fact, it's best that they not even have your number, address or real
name. Know well the schedules and habits of your customers, and
simply call them with very short warning times of your arrival and
readiness to do business. Third parties are not invited, wanted or
allowed. If they don't have all the cash ready at hand, just front the
remainder with an understanding of how long it will take to gather up
the balance. Then return similarly unannounced to collect what is
owed. By this I don't mean to come back in a couple hours to pick up
the marked bills. Rather, the time frame must be sufficiently long so as
to make a stake-out by the enemy a real pain and not worth their
bother.
Explicit telephone conversations with one's customers are a
definite no-no, and such an understanding must be reached with them
from the outset. Rather, the conversations should be friendly, filled
with small talk, and mostly held to make sure the guy is home. Use of
codewords and other such nonsense is for idiots. If one's customer
breaks these pre-agreed-upon rules, it is cause for suspicion.
The delivery machine of choice is a street-legal dirt bike. This
vehicl
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